$19.12
Urine, Artificial (Control) 500ml -IS5070
$5.39
Iodine Potassium Iodide Solution 100ml -IS5501
$18.12
Iodine Potassium Iodide Sol Startch Test 500ml -IS5502
$19.12
Buffer Calibration Kit 500ml -IS5050
$16.91
Staphylococcus Epidermidis Freeze Dried With Transfer Med -IS3906
$20.86
Urine, Artificial W/Vitamin C 500ml -IS5071
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Luminol Blend - For Forensic Detection Of Blood -IS5040
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Tryptic Soy Broth, 100g 25 G/L -IS5133
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In a reaction vessel salicylic acid, acetic anhydride and sulfuric acid are mixed. The exothermic reaction will cause the temperature to increase to 70-80°C. Once the reaction is complete the vessel is cooled in an ice bath and the acetylsalicylic acid crystallizes out. This material is re-crystallized in toluene to purify the product. The product identity is confirmed by melting point. The mass of the re-crystallized product is used to determine the yield of the synthesis. In this experiment, we will perform the synthesis of acetylsalicylic acid (aspirin), purification by re-crystallization and use melting point to confirm identity.
